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BS ISO 23420:2021

BS ISO 23420:2021

$167.15

Microbeam analysis. Analytical electron microscopy. Method for the determination of energy resolution for electron energy loss spectrum analysis

Published By Publication Date Number of Pages
BSI 2021 38
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This document specifies a determination procedure of energy resolution in the scanning transmission electron microscope or the transmission electron microscope equipped with the electron energy loss (EEL) spectrometer.

This document is applicable to both in-column type EEL spectrometer and post-column type EEL spectrometer. These EEL signal detecting systems are applicable to a parallel detecting system and a serial detecting system.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
11 4 Symbols and abbreviated terms
13 5 Definition of the energy resolution
6 Reference materials and energy determination
6.1 General
6.2 Materials selection for energy scale calibration
14 6.3 Binding energy measurement of graphite in the XPS
7 Measurement procedure and energy resolution determination
7.1 General
16 7.2 Predetermination of binding energy
7.2.1 Obtain graphite and the other reference sample
7.2.2 Measure C1s of graphite by using the XPS
7.3 Setup of the S/TEM and the EELS, and sample setting
7.4 First energy step, δE1, calibration
7.4.1 EELS acquisition set-up
7.4.2 Determining the EELS first energy step, δE1
17 7.4.3 Acquisition of carbon K-edge EEL spectrum
7.4.4 Calculate calibrated energy step δE1C
20 7.5 Measurement of peak close to the zero-loss peak, ECZLP, for the other reference sample using energy step δE1
7.5.1 EEL spectrum acquisition of the second reference sample using energy step δE1
21 7.5.2 Obtain the value for CH2 between the zero-loss peak and the peak ECZLP
7.5.3 Calculate the peak ECZLP energy
22 7.6 Second energy step, δE2, calibration
7.6.1 Determining the EELS second energy step, δE2
23 7.6.2 Acquire ECZLP EEL spectrum
7.6.3 Obtain the value for CH3 between the zero-loss peak and peak ECZLP
7.6.4 Calculate calibrated energy step δE2C
7.7 Determining the calibrated EEL spectrometer energy resolution, ΔE
7.7.1 Acquisition of a ZLP EEL spectrum
7.7.2 Obtain the value for CH4 for the zero-loss peak
7.7.3 Calculate EEL spectrometer energy resolution, ΔE
24 7.8 Record items
25 8 Uncertainty for the measurement result of energy resolution
26 Annex A (informative) Example of measurement procedure for energy resolution determination
34 Annex B (informative) Correspondence between energy values of XPS C1s and EELS carbon K edge
36 Bibliography

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BS ISO 23420:2021
$167.15