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BS EN ISO 12183:2024

BS EN ISO 12183:2024

$167.15

Nuclear fuel technology. Controlled-potential coulometric measurement of plutonium

Published By Publication Date Number of Pages
BSI 2024 38
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This document specifies an analytical method for the electrochemical measurement of pure plutonium nitrate solutions of nuclear grade, with an expanded uncertainty not exceeding ±0,2 % at the confidence level of 0,95 for a single determination (coverage factor, k = 2). The method is applicable for aqueous solutions containing plutonium at more than 0,5 g/l and test samples containing plutonium between 4 mg and 15 mg. Application of this technique to solutions containing plutonium at less than 0,5 g/l and test samples containing plutonium at less than 4 mg requires experimental demonstration by the user that applicable data quality objectives will be met.

PDF Catalog

PDF Pages PDF Title
2 undefined
14 7.1 Plutonium determination
20 7.2 Analysis of subsequent test samples
8.1 Calculation of the electrical calibration factor
21 8.2 Calculation of the blank
8.3 Fraction of electrolysed plutonium
22 8.4 Plutonium, amount of substance and mass
8.5 Quality control
23 9.1 Repeatability
9.2 Confidence interval
9.3 Analysis time
27 11.1 Accountability measurements and reference material preparation
11.2 Process control measurements
28 11.3 Measurement cell design
11.4 Electrolyte and electrode options
11.5 Test sample size
29 11.6 Background current corrections
11.7 Correction for iron
30 11.8 Control-potential adjustment
31 11.9 Calibration methodologies

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BS EN ISO 12183:2024
$167.15