BS EN 17194:2019:2020 Edition
$167.15
Animal feeding stuffs: Methods of sampling and analysis. Determination of Deoxynivalenol, Aflatoxin B1, Fumonisin B1 & B2, T-2 & HT-2 toxins, Zearalenone and Ochratoxin A in feed materials and compound feed by LC-MS/MS
Published By | Publication Date | Number of Pages |
BSI | 2020 | 36 |
This document’s method of analysis is applicable for the determination of:
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deoxynivalenol (DON) in the tested range of 100 μg/kg to 3 300 μg/kg,
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aflatoxin B1 (AfB1) in the tested range of 2,5 μg/kg to 440 μg/kg,
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fumonisin B1 (FB1) in the tested range of 690 μg/kg to 7 500 μg/kg,
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fumonisin B2 (FB2) in the tested range of 200 μg/kg to 2 500 μg/kg,
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T-2 toxin in the tested range of 7,5 μg/kg to 360 μg/kg,
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HT-2 toxin in the tested range of 14 μg/kg to 1 800 μg/kg,
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zearalenone (ZEN) in the tested range of 30 μg/kg to 600 μg/kg, and
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ochratoxin A (OTA) in the tested range of 10 μg/kg to 230 μg/kg
in cereals and cereal-based compound feed by liquid-chromatography tandem mass spectrometry (LCMS/ MS). The actual working ranges could extend beyond the tested ranges.
PDF Catalog
PDF Pages | PDF Title |
---|---|
2 | undefined |
6 | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle |
7 | 5 Reagents |
9 | 6 Apparatus |
10 | 7 Procedure 7.1 Sample preparation |
11 | 7.2 Extraction 7.2.1 Introduction 7.2.2 Dry samples 7.2.3 Slurry 7.3 Test solution |
12 | 7.4 Spiking procedure 8 Measurements 8.1 General 8.2 LC conditions 8.3 MS conditions |
13 | 8.4 Batch composition 8.5 Peak identification 8.6 Determination of mycotoxins in calibration and test solutions 8.7 Calibration |
14 | 9 Determination of mass fraction |
15 | 10 Precision 10.1 Interlaboratory study 10.2 Repeatability |
16 | 10.3 Reproducibility 11 Test report |
17 | Annex A (informative)Precision data |
27 | Annex B (informative)Examples B.1 General B.2 Example 1 B.2.1 General B.2.2 LC conditions |
28 | B.2.3 MS conditions |
29 | B.3 Example 2 B.3.1 General B.3.2 LC conditions |
30 | B.3.3 MS conditions |
32 | Annex C (informative)Example chromatograms |